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›› 2001, Vol. 1 ›› Issue (4): 0-0.

• 4 •    

聚乙二醇修饰的高分子磁性微球的合成及表征

姜波,官月平,王靖,刘会洲   

  1. 中国科学院化工冶金研究所分离科学和工程青年实验室及生化工程国家重点实验室, 北京100080
  • 出版日期:2001-08-20 发布日期:2001-08-20

Self-assembly of the [60]fullerene-substituted Oligopyridines on Au Surface

LIU Hui-biao, LI Yu-liang, LUO Hong-yuan, ZHU Dao-ben   

  1. Youth Lab. Sep. Sci. & Eng., State Key Lab. Biochem. Eng., Inst. Chem. Metall., CAS, Beijing 100080, China
  • Online:2001-08-20 Published:2001-08-20

摘要: 利用显微摄相、红外光谱、激光粒度分析等手段对所合成的聚乙二醇(PEG)修饰的四氧化三铁/聚乙烯醇(PVA)磁性高分子微球的形貌、结构组成、磁响应性、酸碱稳定性以及温度稳定性进行了表征. 结果表明, 所合成高分子磁性微球的粒度分布较窄,具有超顺磁性和较强的磁响应性. 微球被PEG有效功能化,在三相相转移催化和生物技术领域中具有良好的应用前景.

关键词: 磁性, 高分子微球, 聚乙二醇修饰, 聚乙烯醇, 合成, 表征

Abstract: PEG-modified Fe3O4/PVA magnetic polymer micropheres were synthesized and characterized by microphotography, laser diffraction particle analysis, FT-IR spectroscopy etc. The results indicate that the size of micropheres presents a Gaussian distribution, and PEG could be immobilized to PVA magnetic microspheres. The magnetic polymer microspheres are stable in a wide range of pH and temperature. The contents of PEG and Fe3O4 were about 190 mg/g and 100 mg/g in the microspheres respectively. These properties make the microspheres promising in applications in the field of catalysis and biotechnology.

Key words: fullerene, gold nanoparticles, self-assembled monolayer

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