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过程工程学报 ›› 2016, Vol. 16 ›› Issue (3): 529-532.DOI: 10.12034/j.issn.1009-606X.215406

• 材料工程专栏 • 上一篇    下一篇

用激光粒度分析仪检测细粒径SiO2基相变调湿复合材料的粒度分布

张浩 刘秀玉 宗志芳 朱庆明 杜晓燕 林晓飞   

  1. 安徽工业大学建筑工程学院 安徽工业大学建筑工程学院 安徽工业大学建筑工程学院 安徽工业大学建筑工程学院 安徽工业大学建筑工程学院 安徽工业大学建筑工程学院
  • 收稿日期:2015-12-09 修回日期:2016-01-13 出版日期:2016-06-20 发布日期:2017-04-28
  • 通讯作者: 张浩

Particle Distribution Measurement of SiO2-based Phase Change and Humidity Controlling Composite Material with Fine Particle Size by Laser Particle Size Analyzer

ZHANG Hao LIU Xiu-yu ZONG Zhi-fang ZHU Qing-ming DU Xiao-yan LIN Xiao-fei   

  1. School of Civil Engineering and Architecture, Anhui University of Technology School of Civil Engineering and Architecture, Anhui University of Technology School of Civil Engineering and Architecture, Anhui University of Technology School of Civil Engineering and Architecture, Anhui University of Technology School of Civil Engineering and Architecture, Anhui University of Technology School of Civil Engineering and Architecture, Anhui University of Technology
  • Received:2015-12-09 Revised:2016-01-13 Online:2016-06-20 Published:2017-04-28
  • Contact: ZHANG Hao

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被引次数

3

摘要： 以SiO2为载体、棕榈醇-棕榈酸-月桂酸为相变材料，采用溶胶-凝胶法制备细粒径SiO2基相变调湿复合材料，以中位径(d50)为评价指标，采用激光粒度分析仪研究了溶液溶质浓度、超声时间、超声频率及分散介质对材料粒度的影响. 结果表明，激光粒度分析仪可用于检测SiO2基相变调湿复合材料的粒度分布，水对材料的分散效果比乙醇好，以水为分散介质，材料最佳溶质浓度为5~10 g/L，最佳超声时间为15 min以上，最佳超声功率大于400 W.

关键词: 激光粒度分析, SiO2基相变调湿复合材料, 粒度分布, 中位径, 检测条件

Abstract: Using SiO2 as the carrier and hexadecanol-palmitic acid-lauric acid as a phase change material, SiO2-based phase change and humidity controlling composite materials were prepared by the sol-gel process. The effects of solute concentration, ultrasonic time, ultrasonic power and dispersing medium on the particle size measurements were investigated by using median particle diameters (d50) as an evaluation indicator. The results indicated that the laser particle size analyzer (test range 1~10000 nm) is applicable to the particle size measurement of SiO2-based phase change and humidity controlling composite materials showing high reproducibility. The dispersion effect of water is better than that of alcohol. When the solute concentrationwas 5~10 g/L, the needed ultrasonic time was longer than 15 min and ultrasonic power was higher than 400 W, optimum dispersion results of SiO2-based phase change and humidity controlling composite materials can be achieved using water as the dispersing medium.

Key words: laser particle size analysis, SiO2-based phase change and humidity controlling composite materials, particle size distribution, median particle diameters, dispersing condition

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